The Tertiary rocks of NE India host number of oil and gas reserves which is an indication for the presence of good source rocks capable of generating such a prolific accumulation of oil and gas in the region. Twenty five oil shale samples collected from Palaeogene outcrops (Disang Group) of the study area were analyzed using Rock-Eval-VI. In addition, two oil-seep samples (Barail Group) have also been analyzed for their geochemical characteristics. The study reveals that the hydrocarbons in both the oil shales and the oil-seeps are in an immature stage and genetically relate to terrestrial sources.