14-membered demi-macrocyclic ligand incorporating N2O2 donor has been kinetically studied in region on a varion carry 50 UV spectrophotometer under pseudo first-order conditions in the pH range 6.55. Both the nature of ligand substituents as well as the size of demi-macrocyclic ring influence relative stability of complex. The determined rate constant was found excellent giving yield more than 80%.
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